3D printed tetrakis(triphenylphosphine)palladium (0) impregnated stirrer devices for Suzuki–Miyaura cross-coupling reactions
نویسندگان
چکیده
In a novel approach, SLA 3D-printed Pd(PPh 3 ) 4 containing stirrer beads have been used to catalyse the Suzuki–Miyaura reaction between range of substrates.
منابع مشابه
Alkylboron Cross-Coupling Reactions
The ability to append alkyl moieties onto preexisting molecular scaffolds is of significant interest owing to the breadth of the diversified compounds that can be accessed in late stage synthesis. There are a number of procedures that are capable of incorporating alkyl subunits into organic molecules; however, many of these strategies are limited in scope. In particular, the highly reactive nat...
متن کامل3D Printed Paper-Based Microfluidic Analytical Devices
As a pump-free and lightweight analytical tool, paper-based microfluidic analytical devices (μPADs) attract more and more interest. If the flow speed of μPAD can be programmed, the analytical sequences could be designed and they will be more popular. This reports presents a novel μPAD, driven by the capillary force of cellulose powder, printed by a desktop three-dimensional (3D) printer, which ...
متن کامل3D Printed Graphene Based Energy Storage Devices
3D printing technology provides a unique platform for rapid prototyping of numerous applications due to its ability to produce low cost 3D printed platforms. Herein, a graphene-based polylactic acid filament (graphene/PLA) has been 3D printed to fabricate a range of 3D disc electrode (3DE) configurations using a conventional RepRap fused deposition moulding (FDM) 3D printer, which requires no f...
متن کامل3D-printed devices for continuous-flow organic chemistry
We present a study in which the versatility of 3D-printing is combined with the processing advantages of flow chemistry for the synthesis of organic compounds. Robust and inexpensive 3D-printed reactionware devices are easily connected using standard fittings resulting in complex, custom-made flow systems, including multiple reactors in a series with in-line, real-time analysis using an ATR-IR ...
متن کاملIron-catalyzed cross-coupling reactions.
Simple iron salts such as FeCl(n), Fe(acac)(n) (n = 2,3) or the salen complex 4 turned out to be highly efficient, cheap, toxicologically benign, and environmentally friendly precatalysts for a host of cross-coupling reactions of alkyl or aryl Grignard reagents, zincates, or organomanganese species with aryl and heteroaryl chlorides, triflates, and even tosylates. An "inorganic Grignard reagent...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ژورنال
عنوان ژورنال: Reaction Chemistry and Engineering
سال: 2023
ISSN: ['2058-9883']
DOI: https://doi.org/10.1039/d2re00218c